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KMID : 0881720220370030129
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Journal of Food Hygiene and Safety
2022 Volume.37 No. 3 p.129 ~ p.135
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Development of Rapid Analytical Method for Heavy Metals (Cd, Pb) in Meju using fs LA-ICP-MS
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Shin Hee-Chang
Choi Ji-Hye
Kim Yong-Kyoung
Kim Dae-Jung
An Jae-Min
Kim Sung-Youn
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Abstract
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The official analytical method for the analysis of harmful heavy metals in Meju, distributed in Korea, employs a strong acid to decompose the organic components. This analysis is time consuming and harmful to the users and/or the environment. This study aimed to develop a new pre-treatment technology using laser ablation, to rapidly analyze harmful heavy metals without using strong acids. The results obtained from this method were validated by the National Institute of Food and Drug Safety Evaluation guideline (NIFDS, 2016). Moreover, a comparison of the two methods showed that the analytical time for 55 Meju samples was shortened by 96% or more in the new method. The results showed no significant difference in the recovery ranging from 90?120%. The proposed method proved suitable for detecting harmful heavy metals in Meju.
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KEYWORD
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fs LA-ICP-MS, ICP-MS, Heavy metal, Meju, Rapid analytical method
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